International content

  • G-5

        3,6-DIMETHOXY-4-(2-AMINOPROPYL)BENZONORBORNANE SYNTHESIS: A solution of 3.70 g 3,6-dimethoxy-4-formylbenzonorbornane (see under 2C-G-5 for its preparation) in 20 g nitroethane was treated with 0.88 g anhydrous ammonium acetate...

  • G-4

          2,5-DIMETHOXY-3,4-(TETRAMETHYLENE)AMPHETAMINE; 6-(2-AMINOPROPYL)-5,8-DIMETHOXYTETRALIN SYNTHESIS: A solution of 1,4-dimethoxy-5,6,7,8-tetrahydro-beta-naphthaldehyde (see preparation under 2C-G-4) in 20 mL nitroethane was treated with 0.13 g anhydrous ammonium acetate and...

  • G-3

        2,5-DIMETHOXY-3,4-(TRIMETHYLENE)AMPHETAMINE; 5-(2-AMINOPROPYL)-4,7-DIMETHOXYINDANE SYNTHESIS: A solution of 3.7 g of 2,5-dimethoxy-3,4-(trimethylene)benzaldehyde (see preparation under 2C-G-3) in 15 mL nitroethane was treated with 0.7 g anhydrous...

  • FLEA

        N-HYDROXY-N-METHYL-3,4-METHYLENEDIOXYAMPHETAMINE SYNTHESIS: (from 3,4-methylenedioxyphenylacetone) A solution of 2.1 g N-methylhydroxylamine hydrochloride and 4.4 g 3,4-methylenedioxyphenylacetone in 5.5 mL MeOH was added to a suspension...

  • F-22

    6-(2-AMINOPROPYL)-2,2-DIMETHYL-5-METHOXY-2,3-DIHYDROBENZOFURAN SYNTHESIS: To a solution of 43.2 g flaked KOH in 250 mL hot EtOH there was added 96 g 4-methoxyphenol followed by 90 g 2-methylallyl...

  • F-2

    6-(2-AMINOPROPYL)-5-METHOXY-2-METHYL-2,3-DIHYDROBENZOFURAN SYNTHESIS: To a solution of 43.2 g KOH pellets in 250 boiling EtOH there was added 96 g 4-methoxyphenol followed by the slow addition of...

  • ETHYL-K

         2-ETHYLAMINO-1-(3,4-METHYLENEDIOXYPHENYL)PENTANE; N-ETHYL-1-(1,3-BENZODIOXOL-5-YL)-2-PENTYLAMINE SYNTHESIS: A solution of 120 mg mercuric chloride in 160 mL H2O was poured over 4.7 g aluminum foil (Reynolds Wrap, regular...

  • ETHYL-J

        2-ETHYLAMINO-1-(3,4-METHYLENEDIOXYPHENYL)BUTANE; N-ETHYL-1-(1,3-BENZODIOXOL-5-YL)-2-BUTANAMINE SYNTHESIS: A stirred solution of 9.0 g 1-(3,4-methylenedioxyphenyl)-2-butanone (see the recipe for J for its preparation) in 150 mL MeOH was treated...

  • EMM

        4,5-DIMETHOXY-2-ETHOXYAMPHETAMINE SYNTHESIS: A solution of 166 g 3,4-dimethoxybenzaldehyde in 600 mL acetic acid was well stirred, and brought up to an internal temperature of...

  • EME

        2,5-DIETHOXY-4-METHOXYAMPHETAMINE SYNTHESIS: To a solution of 14.0 g 4-ethoxy-3-methoxyphenol (see the recipe for MME for the preparation of this starting material) in an equal...

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