International content
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J; BDB
2-AMINO-1-(3,4-METHYLENEDIOXYPHENYL)BUTANE; 1-(1,3-BENZODIOXOL-5-YL)-2-BUTANAMINE SYNTHESIS: The Grignard reagent of propyl bromide was made by the dropwise addition of 52 g 1-bromopropane to a stirred suspension of...
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IRIS
5-ETHOXY-2-METHOXY-4-METHYLAMPHETAMINE SYNTHESIS: To a solution of 9.5 g flaked KOH (10% excess) in 500 mL 95% EtOH there was added 20.4 g 4-methoxy-2-methylphenol (see...
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IP
ISOPROSCALINE; 3,5-DIMETHOXY-4-(i)-PROPOXYPHENETHYLAMINE SYNTHESIS: A solution of 5.8 g of homosyringonitrile (see under ESCALINE for its preparation) and 13.6 g isopropyl iodide in 50 mL...
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IM
ISOMESCALINE; 2,3,4-TRIMETHOXYPHENETHYLAMINE SYNTHESIS: A solution of 8.0 g 2,3,4-trimethoxybenzaldehyde in 125 mL nitromethane containing 1.4 g anhydrous ammonium acetate was held at reflux for...
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IDNNA
2,5-DIMETHOXY-N,N-DIMETHYL-4-IODOAMPHETAMINE SYNTHESIS: To a stirred solution of 0.4 g 2,5-dimethoxy-4-iodoamphetamine hydrochloride (DOI) in 12 mL MeOH containing 4 mL of a 40% formaldehyde solution...
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HOT-17
2,5-DIMETHOXY-4-(s)-BUTYLTHIO-N-HYDROXYPHENETHYLAMINE SYNTHESIS: To a well-stirred solution of 6.08 g 2,5-dimethoxy-4-(s)-butylthio-beta-nitrostyrene (see under 2C-T-17 for its preparation) in 80 mL anhydrous THF under a He atmosphere, there...
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HOT-7
2,5-DIMETHOXY-N-HYDROXY-4-(n)-PROPYLTHIOPHENETHYLAMINE SYNTHESIS: A well-stirred solution of 1.77 g 2,5-dimethoxy-beta-nitro-4-(n-propylthio)styrene (see under 2C-T-7 for its preparation) in 20 mL anhydrous THF was placed in an He atmosphere...
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HOT-2
2,5-DIMETHOXY-4-ETHYLTHIO-N-HYDROXYPHENETHYLAMINE SYNTHESIS: A solution of 5.50 g 2,5-dimethoxy-4-ethylthio-beta-nitrostyrene (see under 2C-T-2 for its preparation) was made in 80 mL boiling anhydrous THF. On cooling, there was...
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G-N
1,4-DIMETHOXYNAPHTHYL-2-ISOPROPYLAMINE SYNTHESIS: To a solution of 3.9 g 1,4-dimethoxy-2-naphthaldehyde (see under 2C-G-N for the preparation) in 13.5 mL nitroethane there was added 0.7 g anhydrous ammonium...
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GANESHA
2,5-DIMETHOXY-3,4-DIMETHYLAMPHETAMINE SYNTHESIS: A solution of 15.4 g 2,5-dimethoxy-3,4-dimethylbenzaldehyde (see under 2C-G for the preparation) in 50 mL nitroethane was treated with 3 g anhydrous ammonium acetate...