A tropical, coffee-like shrub from the Amazonian lowlands, which is widely cultivated in South America, Hawaii and California as a result of the spreading of...
2-METHOXY-4,5-METHYLENEDIOXYAMPHETAMINE SYNTHESIS: A solution of 11.5 g pellet KOH (85%) in 75 mL EtOH was treated with 25 g sesamol followed by 27 g methyl iodide....
3-METHOXY-4,5-METHYLENEDIOXYAMPHETAMINE SYNTHESIS: (from protocatechualdehyde) A solution of 18 g commercial protocatechualdehyde (3,4-dihydroxybenzaldehyde) in 200 mL warm acetic acid was filtered free of any insolubles, to provide...
2-METHOXY-N-METHYL-4,5-METHYLENEDIOXYAMPHETAMINE SYNTHESIS: A suspension of 17.4 g electrolytic elemental iron in 100 g glacial acetic acid was heated on the steam-bath until there were the first...
PMMA; DOONE; 4-MMA; 4-METHOXY-N-METHYLAMPHETAMINE SYNTHESIS: A solution of 20 g methylamine hydrochloride in 150 mL hot MeOH was treated with 10.0 g 4-methoxyphenylacetone and stirred magnetically....
2-METHYLAMINO-1-(3,4-METHYLENEDIOXYPHENYL)PENTANE; N-METHYL-1-(1,3-BENZODIOXOL-5-YL)-2-PENTYLAMINE SYNTHESIS: The Grignard reagent of butyl bromide was prepared in anhydrous Et2O by the dropwise addition of 68 g n-butyl bromide to a well-stirred...
2-METHYLAMINO-1-(3,4-METHYLENEDIOXYPHENYL)BUTANE; N-METHYL-1-(1,3-BENZODIOXOL-5-YL)-2-BUTANAMINE SYNTHESIS: A solution of 0.12 g mercuric chloride in 180 mL H2O was added to 5 g aluminum foil that had been cut into...
4-BROMO-2,5-DIMETHOXY-N-METHYLAMPHETAMINE SYNTHESIS: To a solution of 6.0 g of the free base of 2,5-dimethoxy-N-methyl-amphetamine (see recipe under METHYL-DMA) in 30 mL glacial acetic acid there was...
DMMA; 2,5-DIMETHOXY-N-METHYLAMPHETAMINE SYNTHESIS: To a stirred solution of 28.6 g methylamine hydrochloride in 120 mL MeOH there was added 7.8 g 2,5-dimethoxyphenylacetone followed by 2.6 g...
2,4-DIMETHOXY-5-METHYLTHIOAMPHETAMINE SYNTHESIS: To 27 g 1,3-dimethoxybenzene that was being well stirred, there was added, dropwise, 29 g concentrated H2SO4 over a period of 15 min. Stirring...